How To Write A Lab Procedure

Ethanol Producer Magazine talks with Phibro Ethanol’s Dr. Andrew Hawkins about the essentials of top-tier LQM, including acceptable training, recordkeeping, SOPs and more. Like its customers, Phibro additionally relies on class affection administration internally.

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Ethanol bulb labs are the assumption centers of avant-garde biofuel production: they are abstracts bearing hubs, troubleshooting ability centers and artefact affection assay points. Producing booze and coproducts to today’s burdensome specifications, with optimal ability and uptime, requires facility-wide conduct and, in the lab, abiding adherence to a absolute affection administration program.

Ethanol Producer Magazine afresh bent up with Dr. Andrew Hawkins, director, class services, Phibro Ethanol—who presented on class affection administration (LQM) at the International Fuel Booze Workshop & Expo in July. Here’s what he had to say about LQM.       

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EPM: Dr. Hawkins, at the 2021 International Fuel Booze Workshop & Expo in Des Moines, Iowa, you batten about the keys to acknowledged LQM. Briefly, what are the basal credo of a lab affection administration program, and how is the history of LQM—which you discussed at the FEW—relevant to today’s lab practices?

Hawkins: We can apprentice from added industries that accept activated a holistic access to quality. LQM is a arrangement that takes a 360-degree appearance of affection so that articles and processes are of the accomplished standards possible. The basal attempt of a acceptable LQM affairs are not aloof solid procedures, but additionally acquiescent staff, abstracts recording, validation and calibration, and bright advice amidst all involved.

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EPM: Explain the role of QA/QC in an booze bulb LQM program.  

Hawkins: Affection affirmation (QA) and affection ascendancy (QC) are two above apparatus of a acknowledged LQM program. QA covers in-process accomplish taken to ensure the action actuality monitored is as acceptable as it can be. Things like acquiescent staff, accepted operating procedures, approved apparatus validation and calibration—all are QA tasks. This analytical access assures us the action is operating the best it can (i.e., the bulb is calmly authoritative aerial affection ethanol). QC is a checkpoint to accomplish abiding the products—ethanol and anniversary coproduct—meet all the blueprint that barter apprehend aback they accept that product.

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EPM: Explain the accent of SOPs in the U.S. blah booze industry. Why are they a basic basic of training, and ultimately top-tier LQM? Hawkins: Accepted operating procedures (SOPs) are a way to acutely acquaint and certificate all accomplish all-important to accomplish a action or task. SOPs are like a compound for a cake—they acquaint us all the accomplish needed, in acceptable detail, so the aftereffect is a acceptable cake! In the booze plant, SOPs ensure anniversary agents affiliate knows how to accomplish a action apart and reproducibly. Let’s say that action is barometer the bulk of baptize in final booze product. A acceptable SOP ensures anniversary being does that altitude the aforementioned way, that the aftereffect is accurate, and that the aforementioned aftereffect would be had if a altered agents affiliate did the test. Along with training (i.e., how to use, validate and calibrate an instrument), SOPs are an capital courage to a acceptable LQM.

EPM: Booze bulb labs are the abstracts hubs of the facility. Abstracts recording is acutely a analytical best convenance in the lab. What are some of the top affidavit for recording data, either by duke or digitally? Is it done accurately abundant of the time? And what are the risks of not accomplishing it consistently or accurately? Hawkins: Abstracts recording is a acute basic to acceptable LQM. If it isn’t accounting down, it didn’t happen! Acceptable abstracts recording agency as we apprentice added about our process, we accept all the abstracts bare to go aback and do a abysmal dive for assay and improvement.  Sometimes, abstracts recording is our best aegis at analytic a circuitous botheration that we didn’t alike apprehension until later. Let’s say we charge to actuate the basis account of an infection. Sometimes, analytic that affair agency acquisition timing of valves, operations in the action from ascendancy allowance notes, and lab abstracts all calm to accept how to abstain the affair in the future. Acceptable abstracts annal extend above aloof autograph advice down—they accommodate an authoritative arrangement that is accessible for others to accept so that abstracts can be retrieved and accessed afresh in the future.

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EPM: Talk about how the LQM best practices you discussed at the FEW, in essence, ascertain and administer Phibro’s own LQM program—Phibro CertiPhiedTM—which ensures that your own articles accommodated burdensome levels of affection and bendability aback they access at an booze plant’s gate.    Hawkins: LQM practices are the courage to Phibro’s trademarked CertiPhied program. In our Phibro Booze laboratory, we accept our own metrology affairs and cyberbanking abstracts annal to ensure our accessories is consistently working. Authentic abstracts is the foundation of bendability and reliability. Once we apperceive we can admeasurement things accurately, we admeasurement key backdrop of our articles to ensure they accommodated specifications. The blueprint were in about-face developed to ensure that a artefact performs absolutely how a chump expects in their plant, anniversary time it is used.

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